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Thermoplastic starch (TPS) films added with mucilage from opuntia ficus indica: Mechanical, microstructural and thermal characterization

TitleThermoplastic starch (TPS) films added with mucilage from opuntia ficus indica: Mechanical, microstructural and thermal characterization
Publication TypeArticolo su Rivista peer-reviewed
Year of Publication2020
AuthorsScognamiglio, F., Mirabile Gattia Daniele, Roselli G., Persia F., Angelis U., and Santulli C.
JournalMaterials
Volume13
ISSN19961944
KeywordsBio-plastics, Blending, Cactus mucilage, Differential scanning calorimetry, Extraction, Extraction process, Mechanical performance, Plasticization effects, Reinforced plastics, Salts, Scanning electron microscopy, starch, Tensile testing, Thermal characterization, Thermoplastic starch, Thermoplastic starch films
Abstract

Opuntia cladodes are a typical vegetable waste, from which mucilage in gel form can be extracted. This work proposes blending it with a self-produced thermoplastic starch (TPS), originating from potato starch with a high content in glycerol (ca. 30%). Three methods were compared for extraction, bare maceration (MA), mechanical blending (ME) and mechanical blending following maceration (MPM) to produce films with an approximate thickness of 150 μm. For the comparison, tensile testing, differential scanning calorimetry and scanning electron microscopy were used. The MPM process proved the most effective, not only for extraction yielding, but also to obtain a larger deformation of the samples with respect to the one allowed by the pure TPS films. A considerable plasticization effect was observed. Despite this, the mechanical performance is still not completely satisfactory, and the expected effect of the calcium and magnesium salts contained in the mucilage to improve the rigidity of the TPS film was not really revealed. Prospected improvements would concern the fabrication process and the investigation of other possible loading modes and sample geometries. © 2020 by the authors.

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URLhttps://www.scopus.com/inward/record.uri?eid=2-s2.0-85082017866&doi=10.3390%2fma13041000&partnerID=40&md5=67f8f070b9e6e814d2f1d8e7eb9b8500
DOI10.3390/ma13041000
Citation KeyScognamiglio2020